International Journal of Modern Science and Technology
International Journal of Modern Science and Technology, Vol. 2, No. 1, 2017, Pages 13-19.
Investigations on Transport and Magnetic Properties of Pb (0.1) Doped LaMnO3 Single Crystals
M. Ramesh Babu1,2, P. Kokila1, R. Jayavel2
1Department of Physics, Arulmigu Palaniandavar College of Arts and Culture, Palani. Tamil Nadu, India.
2Crystal Growth Centre, Anna University, Chennai – 600025. Tamil Nadu, India.
*Corresponding author’s e-mail: rameshbabucgc@gmail.com
Abstract
Single crystals of La0.9Pb0.1MnO3 (LPMO) were grown from the flux solution of PbF2 and PbO. The X ray back reflection Laue pattern and powder diffraction were carried out to determine quality and structure of the grown LPMO single crystals. Surface morphology and the chemical composition of the grown crystals were studied using SEM and EDX. Resistivity measurement was performed in a magnetic field of 0T and 6T and its magneto-resistance value was determined. Hysteresis was measured using magnetic field parallel and perpendicular to ‘ab’ plane at 10K. DC magnetization was carried out between the temperature ranges 10 K-300 K. The magnetic field dependence of ZFC and FC condition magnetization were measured with the field at 20 Oe and 500 Oe.
Keywords: Olossal magnetoresistance; Single crystals; Surface morphology; Cluster glass.
References
- Carlos M, Octavio P. Recent advances in perovskites: Processing and properties. Progress in Solid State Chemistry. 2015;43:123-148.
- Litvinchuk AP, Iliev MN, Chu CW, Gospodinov M. Optical properties of magnetoresistive La0.7Pb0.3MnO3 single crystals. Physica C. 2000;341-348:2237-2238.
- Banerjee A, Chaudhuri BK, Sarkar A, Sanyal D, Banerjee D Positron annihilation studies on the La1-xPbxMnO3 system. Physica B.2001;299:130-134.
- Ben Hassine A, Dhahri A, Bouazii ML, Ouezzine M, Hlil EK. Effect of trivalent rare earth doping on magnetic and magnetocaloric properties of La0.47(Y,Eu)0.2Pb0.33MnO3manganites. Ceramics Internationals. 2017;43:1390-1393.
- Zaidi N, Mnefgui S, Dhahri A, Dhahri J, Hlil EK. Study of electrical transport and magnetoresistive properties of La0.67_x DyxPb0.33 MnO3 (x = 0.00, 0.10 and 0.15). Journal of Alloys and Compounds. 2014;616 :378–384.
- Mahendiran R, Mahesh R, Raychaudhuri AK, Rao CNR Room temperature giant magnetoresistance in La1-xPbxMnO3. J Phys Appl Phys D. 1995;28:1743-1745.
- Vogel EM, Fleming JW Preparation of La1-xPbxMnO3 single crystals by high purity melting technique. J Crystal Growth. 1975;29:234-236.
- Ting-Sheng H, Chiung-Hsiung C, Ming-Fong T. Studies on Crystal Structure and Magnetic Scaling Behavior of Perovskite-Like (La1-xPbx)MnO3 System with x = 0 - 0.5. Mat. Res Soc Symp Proc. 2001;674:U 3.4.1-U 3.4.6.
- Prabhakaran D, Boothrhoyd AT. Single-crystal growth of La2−2xSr1+2xMn2O7 under pressure. J Mater Sci. 2003;14:587-589.
- Lin CT, Yan Y, Bischoff E, Peters K, Schonherr E. Lead-doped single crystals of Ln1-x-ySrxPbyMnO3. J Appl Phys. 1999;85:5393-5395.
- Nilotpal Ghosh, Padmanabhan B, Suja Elizabeth, Bhat HL. Surface morphological study of flux grown lead doped rare-earth manganite single crystals. J Crystal Growth. 2005;275:e163-e167.
- Lutteroti L. MAUD Materials Analysis using Diffrction. Version: 1.84 (2002).
- Chernov AA. Crystal Growth and Crystallography Acta Cryst. 1998:A54:859-872.
- Vander Earden JP, Bruinsma OSL. Science and Technology of Crystal Growth. Kulwar Academic. London. 1995.
- Zhiming Wanga, QingyuXu, GangNi, HeZhang. Magnetic entropy change in perovskite Manganites La0.6Pr0.1Pb0.3MnO3 with double metal–insulator peaks. Physica B. 2001;406:4333-4337.
- Shi JB, Fan YY, Tai MF, Chen HZ, Young SL. Magnetic behavior in the La0.7Pb0.3Mn1CoxO3 perovskite compounds. Journal of Magnetism and Magnetic Materials. 2002;239:8-10.
- Kawamura H, Taniguchi T. Chapter 1- Spin Glasses. Handbook of Magnetic Materials. 2015;24:1-137.
- Heilman AK, Xue YY, Ixxrenz B, Gospodino U, Dobreva SG, Chu CW. Field-induced crossover in La0.7Pb0.3MnO3. Physica C. 2000;341-348:707-710.
- Murakami Y, Yoo JH, Shindo D, Atou T, Kikuchi M. Magnetization distribution in the mixed-phase state of hole-doped manganites. Nature. 2003;423:965-968.
- Phan TL, Min SG, Phan MH, Ha ND, Chau N, Yu SC. ESR study of La1-xPbxMnO3 (0.1 x 0.5) perovskites. Phys Stat Sol B. 2007;244:1109-1117.
- Volkov N, Petrakovskii G, Boni P, Clementyev E, Patrin K, Sablina K, Velikanov D, Vasiliev A. Intrinsic magnetic inhomogeneity of Eu substituted La0.7Pb0.3MnO3 single crystals. J Magn Magn Mater. 2007;309:1-9.